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 6770 Freezer/Mill
- Cryogenic impact grinder with self contained liquid nitrogen tub and insulated case
- Hold one 6751 or 6771 sample vial for grinding, with the capacity to hold two additional vials in a pre cooling chamber
- Equipped with touch screen interface for flexibility and a removable control panel
- Capable of storing up to 10 grinding protocols
- Supplied with a 6754 Extractor/Vial Opener, 6755 Vial Rack, Controller Interconnect Cable (8 in/20.3cm), and power cord
- Grinds samples in the 0.1 gram to 5.0 gram range
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| Specifications |
| Dimensions: | 19.5 in (49.5 cm) x 11 in (27.9 cm) x 13.3 in (33.6 cm) |
| Weight: | 18.0 lbs (8.2 kg) net; 22.0 lbs (9.9kg) gross |
| Voltage: | 115V/60Hz |
| Specifications |
| Dimensions: | 19.5 in (49.5 cm) x 11 in (27.9 cm) x 13.3 in (33.6 cm) |
| Weight: | 18.0 lbs (8.2 kg) net; 22.0 lbs (9.9kg) gross |
| Voltage: | 230V/50Hz |
 6870 Freezer/Mill
- Larger cryogenic impact grinder with self-contained liquid nitrogen tub and insulated case.
- Holds one large capacity 6801 sample vial or four 6751 sample vials for grinding, with the capacity to hold one 6801 vial or four 6751 vials in a pre-cooling chamber.
- Equipped with touch screen interface flexibility and a removable control panel.
- Stores up to 10 grinding protocols.
- Grinds samples in the 1.0 - 100.0 gram range.
- Grinding containers sold separately and liquid nitrogen required for operation.
6820 Autofill option available. MUST Choose Accessory Package 6870S or 6870L At Time of Order. Click on Freezer/Mill Accessories Tab Above For Complete Details. |
| Specifications |
| Dimensions: | 18 in. (46 cm) x 20.5 in. (52 cm) x 21.5 in. (55 cm) |
| Weight: | 42 lbs. net (19 kg) |
| Voltage: | 115 V/60 Hz |
| Specifications |
| Dimensions: | 18 in. (46 cm) x 20.5 in. (52 cm) x 21.5 in. (55 cm) |
| Weight: | 42 lbs. net (19 kg) |
| Voltage: | 230 V/50 Hz |
6814 AutoExtractor
The Model 6814 AutoExtractor is an electrically powered version of our catalog #6754/6804 manual
extractors and vial openers. Cold vials can now be opened easily, making the grinding process more
efficient. In medium to high-throughput laboratory facilities, operator fatigue associated with the manual extractors is eliminated, increasing the speed of sample processing. |
6820 Auto-Fill System for the 6870 Freezer/Mill®
The 6820 Auto-Fill System is designated to automatically maintain the required level of liquid nitrogen within the 6870 Freezer/Mill during operation. The Auto-Fill System is a more efficient and safer way to handle the volume of liquid nitrogen required for processing samples in the 6870 Freezer/Mill. This automated system reduces the loss of liquid nitrogen and saves the time lost when manually filling the reservoir.
The Auto-Fill System requires a cryogenic transfer hose, not included with the 6820 package. These transfer hoses are available in different lengths and can be constructed with different materials. The transfer hose must be configured with a 1/2 inch JIC female flare nut at each end for proper installation. The 6820 system is supplied with a safety relief valve that connects to the liquid nitrogen supply via a 1/2 inch JIC female flare nut.
The Auto-Fill System is available as an option that can be installed when you place an order for a 6870 Freezer/Mill or as a retrofit package for 6870 systems that are already in service.
Please contact SPEX SamplePrep for further details. |
 5200 SPEX SamplePrep Micro Hammer-Cutter Mills
- Rapidly pulverizes anything dry and friable.
- Uses high-speed revolving hammers and serrated grinding chamber lining.
- Extremely effective on dried plants, roots, paper and cloth, soil samples, coal and peat, chemicals, and soft rock.
• Supplied with 12 collection tubes and rack.
• Cleaning tools included.
• Three screens are supplied: 2 mm (#520020); 1.5 mm (#520015); 1.0 mm (#520010). |
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| Micro Hammer-Cutter Mill Accessories |
520002 Screen
0.2 mm perforated steel. |
| Specifications |
| Dimensions: | 10 5/8 in. high, 5 7/8 in. x 11 in. |
| Weight: | 12.6 lbs. Net (5.7 kg) |
| Feed Material Size: | 7 mm MAX |
| Specifications |
| Dimensions: | 10 5/8 in. high, 5 7/8 in. x 11 in. |
| Weight: | 12.6 lbs. Net (5.7 kg) |
| Feed Material Size: | 7 mm MAX |
 5100 Mixer/Mill
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High-energy “shaker” mill.
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Pulverizes and/or homogenizes samples of varying composition.
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Grinding containers constructed with a variety of materials.
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Typically grinds samples in the 0.5 gram to 1.5 gram range.
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Holds three vials of 1/2 in. diameter or two vials of 3/4 in. diameter (length of vials up to 2 1/4 in.).
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For grinding up to 3 ml or blending up to 10 ml.
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Push-button, resettable 30-minute timer on the 5100-115 Mixer/Mill.
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Push-button, resettable 72-minute timer on the 5100-230 Mixer/Mill which is also supplied with a continental European CEE 7/7 two-prong plug.
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| Specifications |
| Dimensions: | 12 in. (33 cm) x 8 in. (20 cm) x 8 in. (20 cm) |
| Weight: | 15.2 lbs. Net (7 kg), 19.8 lbs. Gross (9kg) |
| Specifications |
| Dimensions: | 12 in. (33 cm) x 8 in. (20 cm) x 8 in. (20 cm) |
| Weight: | 15.2 lbs. Net (7 kg), 19.8 lbs. Gross (9kg) |
 8000D Dual Mixer/Mill
- Efficient two-clamp laboratory mill for pulverizing hard, brittle samples.
- Also called a shaker mill or high-energy ball mill.
- Sample sizes in the 10-gram per vial range.
- Reduces samples to analytical fineness.
- Can be utilized for mechanical alloying.
- Features include a variable-range electronic timer, dual clamps for multiple sample capacity, safety interlock system, and forced-air cooling.
- A European CEE 7/7 two-prong plug is supplied with the 8000D-230 systems.
- One or two samples can be processed simultaneously, however if one sample is processed, a second empty vial must be inserted to maintain the balance of the system.
- Accepts grinding/mixing vials from 2 3/8 in. to 3 1/8 in. in length and up to 2 1/4 in. in diameter.
- The 8010 and 8011 adapters permit processing of multiple samples in 1/2 in. x 1 in., 1/2 in. x 2 in., and 3/4 in. x 2 in. vials.
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| Specifications |
| Weight: | 82 lb. [37 kg], 98 lb. (44 kg) |
| Motor: | 1/3 HP, 1725 RPM (115 V/60 Hz) or 1425 RPM |
| Power Cord: | 3-prong grounded plug for 115 V/60 Hz version, |
| Clamp Movement: | 2 1/3 in. back-and-forth, 1 in. side-to-side |
| Clamp Speed: | 1060 [115 V/60 Hz] |
| Voltage: | 115 V/60 Hz (8 amp fuse) |
| Controls: | Start, pause, and stop buttons; programmable timer with digital display, factory-set for 100 min. but extendible to 1000 minutes. |
8000D-230 Mixer/Mill
For 230 V/50 Hz operation. A European CEE 7/7 two-prong plug is supplied with the 8000D-230 systems. |
| Specifications |
| Weight: | 82 lb. [37 kg], 98 lb. (44 kg) |
| Motor: | 1425 RPM [230 V/50 Hz] |
| Power Cord: | 2-prong European plug for 230 V/50 Hz version. |
| Clamp Movement: | 2 1/3 in. back-and-forth, 1 in. side-to-side |
| Clamp Speed: | 875 [230 V/50 Hz] |
| Voltage: | 230 V/50 Hz (4 amp fuse) |
| Controls: | Start, pause, and stop buttons; programmable timer with digital display, factory-set for 100 min. but extendible to 1000 minutes. |
 8000M Mixer/Mill®
- Also called a shaker mill or high-energy ball mill.
- Sample sizes in the 10 gram range for grinding and up to 50 ml for mixing.
- Reduces samples to analytical fineness.
- Can be utilized for mechanical alloying.
- Features include a variable-range electronic timer, safety interlock system, and shock-mounted electric motor for tabletop operation.
- A European CEE 7/7 two-prong plug is supplied with the 8000M- 230 systems.
- Accepts grinding/mixing vials from 13/4 in. to 31/8 in. in length and up to 21/4 in. in diameter.
- The 8010 and 8011 adapters permit processing of multiple samples in 1/2 in. x 1 in., 1/2 in. x 2 in., and 3/4 in. x 2 in. vials.
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| Specifications |
| Dimensions: | 19 in. (48 cm) x 14 in. (36 cm) x 18 in. (46 cm) |
| Weight: | 76 lbs. net (35 kg); 92 lbs. gross (41 kg) |
| Motor: | 1/3 horsepower |
| Clamp Speed: | 1060 [115 V/60 Hz] |
| Voltage: | 115 V/60 Hz |
| Controls: | Start, pause, and stop buttons; programmable timer with digital display, factory-set for 100 min. but extendible to 1000 minutes. |
8000M-230 Mixer/Mill
For 230 V/50 Hz operation. A European CEE 7/7 two-prong plug is supplied with the 8000M-230 systems. |
| Specifications |
| Dimensions: | 19 in. (48 cm) x 14 in. (36 cm) x 18 in. (46 cm) |
| Weight: | 76 lbs. net (35 kg); 92 lbs. gross (41 kg) |
| Motor: | 1/3 horsepower |
| Clamp Speed: | 875 [230 V/50 Hz] |
| Voltage: | 230 V/50 Hz (4 amp fuse) |
| Controls: | Start, pause, and stop buttons; programmable timer with digital display, factory-set for 100 min. but extendible to 1000 minutes. |
 8005 Zirconia Ceramic Vial Set
Vial size 2 1/2 in. diameter x 2 11/16 in. Solid zirconia ceramic vial, cap, and two 1/2 in. balls; seven corprene gaskets. Grinding load approx. 2–8 ml; mixing load approx. 20 ml. |
 8007 Stainless Steel Vial Set
Vial size 2 1/4 in. diameter x 3 in. Vial body and cap liner made of hardened 440C stainless steel. Two 1/2 in. and four 1/4 in. stainless steel balls are included. Set includes screw-on cap
with O-ring to permit wet or dry grinding/mixing. Grinding load 3–10 ml; mixing load approx. 25 ml. |
 8008 Silicon Nitride Vial Set
Vial size 2 1/2 in. diameter x 2 11/16 in. solid silicon nitride vial, cap, and two 1/2 in. balls; seven corprene gaskets. Grinding load approx. 2–8 ml; mixing load approx. 20 ml. |
 8009 Round-Ended Hardened Steel Vial Set.
Vial Size 2 3/8 in. diameter x 3 in. Hardened steel vial body has grinding chamber with rounded ends for more efficient grinding/mixing. Includes screw-on cap and O-ring for wet or dry use; two 1/2 in. and four 1/4 in. steel balls. Grinding load 3–10 ml; mixing load approximately 25 ml. |
 8014 Agate Vial Set for 8000 Series Mixer/Mills
For dry grinding and mixing. Vial size 2-1/4 in. diameter x 2-3/4 in. All-agate vial body, two slip-on caps, two 1/2 in. agate balls, and eight corprene gaskets. Grinding load 3–8 ml; mixing load approximately 20 ml. |
 8002 Plastic Vial for 8000 Series Mixer/Mills
2 1/8 in. diameter x 2 1/2 in. Polystyrene body with plastic screw-on cap. Capacity 135 ml; mixing load approx. 50 ml. For use with 3112 or 8006A plastic balls. Sold in units of 100. |
 8006 Methacrylate Vial Set
2 1/4 in. diameter x 2 5/8 in. Vial body of heavy-gauge methacrylate with methacrylate-lined aluminum screw-on cap. Set includes corprene gasket, two 8006A ( 1/2 in.) and four 3112 ( 3/8 in.) plastic balls. Rugged construction allows grinding of soft materials without metallic contamination. |
8006A Methacrylate Balls
1/2 in. diameter, fits all SPEX SamplePrep plastic vials 3/4 in. diameter and larger. Sold in units of 100. |
 8001 Hardened Steel Vial Set
Vial size 2-1/4 in. diameter x 3 in. Vial body and cap liner of hardened tool steel. Set includes screw-on cap with O-ring to allow wet or dry grinding/mixing, two 1/2 in. and four 1/4 in. steel balls. Grinding load 3–10 ml; mixing load approx. 25 ml. |
8001B Steel Ball Set
Two 1/2 in. and four 1/4 in. steel balls, for SPEX SamplePrep 8001 and 8009 vials. |
 8003 Alumina Ceramic Vial Set
For dry grinding/mixing. Vial size 2-1/4 in. diameter x 2-3/4 in. High purity 99.5% alumina ceramic vial body and two slip-on caps with one 1/2 in. ball; set includes eight corprene gaskets. Grinding load 2–8 ml; mixing load approximately 20 ml. |
8015 Clamp for 8003
Clamps permit slurry grinding in 8003 vial; sold in pairs. One pair required for each 8003. |
 8004 Tungsten Carbide Vial Set
For wet or dry grinding/mixing. Vial size 2-1/4 in. diameter x 2-1/2 in. Tungsten carbide-lined body, two screw-on tungsten-carbide-lined caps, two 7/16 in. tungsten carbide balls, eight corprene gaskets. Grinding load 3–10 ml, mixing load approximately 25 ml. |
| Grinding/Mixing Vial Dimensions | | Vial P/N | Description | Overall Height w/Cap & Gasket (mm) | Height w/o Cap (mm) | OD (mm) | ID (mm) | Volume (ml) | | 3111 | Polystyrene Vial | 27 | 25 | 13.6 | 11.7 | 2.5 | | 3114 | Stainless Steel Vial | 27 | 25 | 12.7 | 11.0 | 2.5 | | 3116 | Polystyrene Vial | 57 | 51 | 13.4 | 10.7 | 5 | | 3117 | Hardened Steel Vial | 27 | 25 | 12.7 | 11.0 | 2.5 | | 3118 | Agate Vial | 43 | 33 | 15.9 | 9.5 | 1.6 | | 3127 | Hardened Steel Vial | 45 | 42 | 14.9 | 12.4 | 5 | | 5004 | Tungsten Carbide Vial | 54 | 48 | 19.0 | 12.5 | 5 | | 6133 | Polystyrene Vial | 54 | 51 | 20.1 | 18.0 | 12 | | 6133 PC | Polycarbonate Vial | 54 | 51 | 20.1 | 18.0 | 12 | | 6134 | Polystyrene Vial | 79 | 76 | 27.9 | 24.9 | 35 | | 6135 | Polystyrene Vial | 78 | 76 | 27.9 | 24.9 | 35 | | 8001 | Hardened Steel Vial | 76 | 64 | 51.1 | 37.8 | 65 | | 8002 | Polystyrene Vial | 72 | 64 | 53.3 | 49.9 | 135 | | 8003 | Alumina Ceramic Vial | 70 | 52 | 51.1 | 37.8 | 45 | | 8004 | Tungsten Carbide Vial | 62 | 50 | 50.7 | 40.6 | 55 | | 8003 | Zirconia Ceramic Vial | 68 | 52 | 57.1 | 38.0 | 45 | | 8006 | Methacrylate Vial | 64 | 60 | 50.9 | 37.9 | 55 | | 8007 | Stainless Steel Vial | 76 | 64 | 50.8 | 37.8 | 65 | | 8008 | Silicon Nitride Vial | 62 | 52 | 57.2 | 37.5 | 45 | | 8009 | Round-End-Hardened Steel Vial | 76 | 42 | 58.8 | 37.9 | 35 | | 8014 | Agate Vial | 70 | 53 | 46.9 | 35.3 | 40 |
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 8010 Multiple-Sample Adapter
Holds seven vials, each 1/2 in. in diameter, for simultaneous running in 8000M Mixer/Mill. Suitable vials include SPEX SamplePrep 3111, 3114, 3116 and 3117. Vials run at one time should be same length. Can be used in 8000D Mixer/Mill with 3116 vials, or with 3111, 3114, and 3117 vials if 8012 adapter is also used. |
 8011 Multiple-Sample Adapter.
Holds four vials, each 3/4 in. in diameter, for simultaneous running in 8000M Mixer/Mill. Suitable vials include SPEX SamplePrep 3118, 3127, 5004 and 6133. Vials run at one time should be same length. Can be used in 8000D Mixer/Mill with 3118, 5004, and 6133 vials. To use 3127 vials in 8000D, 8012 adapter is also necessary. |
 3111 Polystyrene Vial
1/2 in. diameter x 1 in. long. Includes slip-on polyethylene cap. Capacity 2.5 ml; mixing load approx. 1 ml; accepts SPEX SamplePrep 3112 or 3119 plastic balls. Sold in units of 100. |
 3116 Polystyrene Vial
1/2 in. diameter x 2 in. long. Includes slip-on polyethylene cap. Capacity 5 ml; mixing load approx. 2 ml; accepts SPEX SamplePrep 3112 or 3119 plastic balls. Sold in units of 100. |
3116PC Polycarbonate Vial
1/2 in. diameter x 2 in. long. Includes slip-on polyethylene cap. Capacity 5 ml; mixing load
approx. 2 ml; accepts SPEX SamplePrep 3112 or 3119 plastic balls. Sold in units of 100. |
 6133 Polystyrene Vial
3/4 in. diameter x 2 in. long. Includes slip-on polyethylene cap. Capacity 12 ml; mixing load approx. 5 ml; accepts SPEX SamplePrep 3112 or 3119 plastic balls. Sold in units of 100. |
6133PC Polycarbonate Vial
3/4 in. diameter x 2 in. long. Includes slip-on polyethylene cap. Capacity 12 ml; mixing load approx. 5 ml. Sold in units of 100. Accepts SPEX SamplePrep 3112, 3119, and 8006A plastic balls. |
 3114 Stainless Steel Vial Set
1/2 in. diameter x 1 in. long. Made of 303 stainless steel; includes slip-on cap and 1/4 in. stainless steel ball; grinding load 0.2–0.6 ml, mixing load 1 ml. |
 3117 Hardened Tool
1/2 in. diameter x 1 in. long. Made of Worpliss tool steel. Includes slip-on cap and 1/4 in. steel ball. Grinding load 0.2 – 0.6 ml, mixing load 1 ml. Four balls per set. |
 3127 Hardened Tool Steel Vial Set
3/4 in. diameter x 1 7/8 in. long. Made of Worpliss tool steel; includes center cylinder with two slip-on caps and 1/4 in. steel ball. Grinding load 0.5–1.0 ml, mixing load 2 ml. |
 3118 Agate Vial Set
Handmade from flawless Brazilian agate; must be run inside cushioned SPEX SamplePrep 6133 vial (included). Includes stopper and 1/4 in. agate ball (3118A) Grinding load 0.2 – 0.6 ml, mixing load 1 ml. |
 5004 Tungsten Carbide-Lined Vial Set
3/4 in. diameter x 2 1/8 in. long. Includes two slip-on Delrin® caps with tungsten carbide inserts, six disposable methacrylate center cylinders, and two 5/16 in. tungsten carbide balls(5004A). Grinding load 0.5–1.5 ml; mixing load 3 ml. |
8500 Shatterbox®
- Features a cam-activated clamp that requires only moderate hand pressure to secure the grinding dish in the Shatterbox and is adjustable for containers of different heights.
- Perforated metal skirt provides ventilation for continuous operation, and a rubber cover protects against dust.
- Includes an anti-skid wood/rubber floor mount and an extra set of drive belts.
- A European CEE 7/7 two-prong plug is supplied with each 8500-230/50 system.
- Grinding containers are sold separately. Timer is not supplied.
- Most popular “swing mill” in America.
- Most efficient way of grinding up to 100 grams of brittle material to analytical fineness.
- Typical samples include cements, soils, ceramics, slag, rocks, and ores. The Shatterbox has also been used to grind sulfur pellets, pharmaceuticals, dried marsh grass, and many other materials.
- Swings a dish-shaped grinding container with a puck, and often a ring, in a tight high-speed circle.
- Typical grinding time is two minutes or less.
- Resultant particle size well below 200 mesh; with proper grinding aid, less than 10 microns.
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| Specifications |
| Dimensions: | 13 in. (33 cm) x 13 in.(33 cm) x 231⁄2 in. (60 cm) |
| Weight: | 135 lbs. gross (61 kg) |
| Motor: | 1/3 horsepower @ 835 RPM |
| Voltage: | 115 V/60 Hz |
| Controls: | |
8500-230/50 Shatterbox
For 230 V/50 Hz operation. A European CEE 7/7 two-prong plug is supplied with the 8000D-230 systems. A European CEE 7/7 two-prong plus is supplied with each 3630-230 system. |
| Specifications |
| Dimensions: | 13 in. (33 cm) x 13 in.(33 cm) x 231⁄2 in. (60 cm) |
| Weight: | 135 lbs. gross (61 kg) |
| Motor: | 1/3 horsepower @ 835 RPM |
| Voltage: | 230 V/50 Hz |
| Controls: | |
 8530 Shatterbox®
- CE approved model.
- Features a cam-activated clamp that requires only moderate hand pressure to secure the grinding dish in the Shatterbox and is adjustable to secure containers of different heights.
- Soundproof enclosure reduces noise levels below OSHA limits.
- Equipped with a safety interlock system, a variablerange electronic timer with digital display, and lockable casters.
- LCD display with environmentally safe, push-button membrane switch.
- Wide choice of grinding containers
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| Specifications |
| Dimensions: | 19 in. (48 cm) x 19 in. (48 cm) x 40 in. (102 cm) |
| Weight: | 225 lbs. net (102 kg); 246 lbs. gross (112 kg) |
| Motor: | 1/2 horsepower @ 835 RPM |
| Voltage: | 230 V/50 Hz |
8515-230 Shatterbox
For 230 V/50 Hz operation. A European CEE 7/7 two-prong plug is supplied with the 8000D-230 systems. A European CEE 7/7 two-prong plug is supplied. |
| Specifications |
| Dimensions: | 19 in. (48 cm) x 19 in. (48 cm) x 40 in. (102 cm) |
| Weight: | 225 lbs. net (102 kg); 246 lbs. gross (112 kg) |
| Motor: | 1/2 horsepower @ 835 RPM |
| Voltage: | 230 V/50 Hz |
| Shatterbox Grinding Containers | | Cat. No. | Material | Outer Dimensions diameter x height | Weight | Recommended load | Dish | Lid | Parts Ring | Puck | Gasket | | 8501 | Hardened Steel | 17.5 x 7.5 cm | 8 kg | 20-50 ml | x | x | x | x | x | | 8504 | Tungsten Carbide1 | 17.5 x 8 cm | 12.5 kg | 20-60 ml | x | x | x | x | x | | 8505 | Alumina Ceramic1 | 15.2 x 8 cm | 5 kg | 15-40 ml | x | x | | x | x | | 8506 | Zirconia Ceramic1 | 15.2 x 8 cm | 6 kg | 15-40 ml | x | x | | x | x | | 8507 | Hardened Steel2 | 9 x 5.4 cm | 1.9 kg | 5-20 ml | x | x | | x | x | | 8508 | Tungsten Carbide1,2 | 9.2 x 5.9 cm | 3.5 kg | 5-20 ml | x | x | | x | | | 8521 | Hardened Steel | 20.3 x 8.2 cm | 13 kg | 30-100 ml | x | x | x | x | x | 1Tungsten carbide, zirconia ceramic and alumina ceramic are brittle as well as extremely hard, and cannot be guaranteed against chipping or breaking. If handling instructions are followed, these contains will provide years of useful service.
2Smaller tungsten carbide (8505) and steel (8507) grinding containers require 8507R rack for proper use in the 8500 and 8515. |
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 8507R Rack
Holds one or three 8507 or 8508 grinding containers. Rack base assembly and lid included; rack with three grinding containers lifts easily in and out of Shatterbox. Please note that 8507 and 8508 containers cannot be mixed during the same run. |
51793 Shatterbox Drive Belt
Special elastomer O-ring.
NOTE: Drive belts should always be replaced as a set to ensure proper operation, 4 required. |
8525 Transporter
A metal carrying handle equipped with a spring-loaded clamp. Specifically designed to lift and hold all large Shatterbox dishes, while transporting the dishes between the sample preparation area and the Shatterbox. |
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